BMRB Entry 18286
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full, SPARTA
BMRB Entry DOI: doi:10.13018/BMR18286
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Title: Solution structure of de novo designed antifreeze peptide 3
Deposition date: 2012-02-21 Original release date: 2012-10-22
Authors: Bhunia, Anirban
Citation: Bhunia, Anirban. "Solution structure of de no designed anti freeze peptide 3" Not known ., .-..
Assembly members:
entity, polymer, 25 residues, 2483.774 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: TGNVGLSPGLSTALTGFTLV
PVEDH
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 120 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | antifreeze_peptide_3 | 1 |
Entities:
Entity 1, antifreeze_peptide_3 25 residues - 2483.774 Da.
| 1 | THR | GLY | ASN | VAL | GLY | LEU | SER | PRO | GLY | LEU | ||||
| 2 | SER | THR | ALA | LEU | THR | GLY | PHE | THR | LEU | VAL | ||||
| 3 | PRO | VAL | GLU | ASP | HIS |
Samples:
sample_1: antifreeze_peptide_3 0.8 mM; H2O 90%; D2O 10%
sample_conditions_1: pH: 5.0; temperature: 288 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA v1.5, Guntert, Braun and Wuthrich - refinement
NMR spectrometers:
- Bruker Avance 800 MHz
- Bruker Avance 500 MHz