BMRB Entry 25200
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR25200
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Title: 3D structure determination of STARP peptides implicated in P. falciparum invasion of hepatic cells PubMed: 20580741
Deposition date: 2014-09-04 Original release date: 2014-10-07
Authors: Adriana, Bermudez; Martha, Alba; Magnolia, Vanegas; Manuel E., Patarroyo
Citation: Bermudez, Adriana; Alba, Martha Patricia; Vanegas, Magnolia; Patarroyo, Manuel Elkin. "3D structure determination of STARP peptides implicated in P. falciparum invasion of hepatic cells" Vaccine 28, 4989-4996 (2010).
Assembly members:
entity, polymer, 20 residues, 2392.855 Da.
Natural source: Common Name: malaria parasite Taxonomy ID: 5833 Superkingdom: Eukaryota Kingdom: not available Genus/species: Plasmodium falciparum
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
entity: KSMINAYLDKLDLETVRKIH
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 153 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | entity | 1 |
Entities:
Entity 1, entity 20 residues - 2392.855 Da.
| 1 | LYS | SER | MET | ILE | ASN | ALA | TYR | LEU | ASP | LYS | |
| 2 | LEU | ASP | LEU | GLU | THR | VAL | ARG | LYS | ILE | HIS |
Samples:
sample_1: entity8 – 9 mM; trifluoroethanol 30%; trifluoroethanol 70%
sample_conditions_1: temperature: 295 K; pH: 3.7; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
Software:
InsightII, Accelrys Software Inc. - geometry optimization, refinement
NMR spectrometers:
- Bruker DRX 600 MHz