BMRB Entry 4397
Chem Shift validation: AVS_anomalous, AVS_full, LACS
BMRB Entry DOI: doi:10.13018/BMR4397
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Title: Solution Structure of the CX3C Chemokine Domain of Fractalkine
Deposition date: 1999-09-09 Original release date: 1999-11-21
Authors: Handel, T.; Mizoue, L.; Bazan, J.; Johnson, E.
Citation: Mizoue, L.; Bazan, J.; Johnson, E.; Handel, T.. "Solution Structure and Dynamics of the CX3C Chemokine Domain of Fractalkine and Its Interaction with an N-Terminal Fragment of CX3CR1" Biochemistry 38, 1402-1414 (1999).
Assembly members:
fractalkine, polymer, 77 residues, Formula weight is not available
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: recombinant technology Host organism: Escherichia coli
Entity Sequences (FASTA):
fractalkine: MQHHGVTKCNITCSKMTSKI
PVALLIHYQQNQASCGKRAI
ILETRQHRLFCADPKEQWVK
DAMQHLDRQAAALTRNG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 257 |
| 15N chemical shifts | 91 |
| 1H chemical shifts | 514 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | fractalkine | 1 |
Entities:
Entity 1, fractalkine 77 residues - Formula weight is not available
| 1 | MET | GLN | HIS | HIS | GLY | VAL | THR | LYS | CYS | ASN | ||||
| 2 | ILE | THR | CYS | SER | LYS | MET | THR | SER | LYS | ILE | ||||
| 3 | PRO | VAL | ALA | LEU | LEU | ILE | HIS | TYR | GLN | GLN | ||||
| 4 | ASN | GLN | ALA | SER | CYS | GLY | LYS | ARG | ALA | ILE | ||||
| 5 | ILE | LEU | GLU | THR | ARG | GLN | HIS | ARG | LEU | PHE | ||||
| 6 | CYS | ALA | ASP | PRO | LYS | GLU | GLN | TRP | VAL | LYS | ||||
| 7 | ASP | ALA | MET | GLN | HIS | LEU | ASP | ARG | GLN | ALA | ||||
| 8 | ALA | ALA | LEU | THR | ARG | ASN | GLY |
Samples:
sample_1: fractalkine, [U-15N; U-13C], 1.6 mM
sample_cond_1: pH: 5.0; pressure: 1 atm; temperature: 295.5 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 3D 15N-edited NOESY | not available | not available | not available |
| 3D 13C-edited NOESY | not available | not available | not available |
| 4D 13C/13C-edited NOESY | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Bruker DMX 600 MHz
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