BMRB Entry 4656
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR4656
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Title: Design and Solution Structure of a Well-folded Stack of Two Beta-hairpins Based on the Amino-terminal Fragment of Human Granulin A PubMed: 10956026
Deposition date: 2000-10-17 Original release date: 2001-05-10
Authors: Tolkatchev, D.; Ng, A.; Vranken, W.; Ni, F.
Citation: Tolkatchev, D.; Ng, A.; Vranken, W.; Ni, F.. "Design and Solution Structure of a Well-folded Stack of Two Beta-hairpins Based on the Amino-terminal Fragment of Human Granulin A" Biochemistry 39, 2878-2886 (2000).
Assembly members:
GRANULIN_A, polymer, 31 residues, Formula weight is not available
Natural source: Common Name: human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: .
Entity Sequences (FASTA):
GRANULIN_A: VVHCDMEVICPDGYTCCRLP
SGAWGCCPFTQ
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 192 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | GRANULIN A | 1 |
Entities:
Entity 1, GRANULIN A 31 residues - Formula weight is not available
| 1 | VAL | VAL | HIS | CYS | ASP | MET | GLU | VAL | ILE | CYS | ||||
| 2 | PRO | ASP | GLY | TYR | THR | CYS | CYS | ARG | LEU | PRO | ||||
| 3 | SER | GLY | ALA | TRP | GLY | CYS | CYS | PRO | PHE | THR | ||||
| 4 | GLN |
Samples:
sample_1: GRANULIN_A 0.5 mM; sodium acetate, [U-2H], 20 mM; D2O 10%; H2O 90%
sample_2: GRANULIN_A 0.5 mM; sodium acetate, [U-2H], 20 mM; D2O 100%
sample_cond_1: pH: 5.0; pressure: 1 atm; temperature: 288 K
sample_cond_2: pH: 5.0; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | not available | not available |
Software:
X-PLOR v3.1 - refinement, structure solution
NMR spectrometers:
- Bruker DRX 500 MHz
Related Database Links:
| PDB |