BMRB Entry 5291
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5291
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Title: Investigation of Penetratin Peptides. Part 1: The Environment Dependent Conformational Properties of Penetratin and two of its Derivatives PubMed: 11991205
Deposition date: 2002-02-15 Original release date: 2002-03-29
Authors: Czajlik, Andras; Mesko, Eszter; Penke, Botond; Perczel, Andras
Citation: Czajlik, Andras; Mesko, Eszter; Penke, Botond; Perczel, Andras. "Investigation of Penetratin Peptides. Part 1: The Environment Dependent Conformational Properties of Penetratin and two of its Derivatives" J. Pept. Sci. 8, 151-171 (2002).
Assembly members:
12 amino acid long derivative of the third helix of Antennapedia homeodomain, polymer, 12 residues, 1716 Da.
Natural source: Common Name: fruit fly Taxonomy ID: 7227 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Drosophila melanogaster
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
12 amino acid long derivative of the third helix of Antennapedia homeodomain: RQIKIWFRKWKK
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 119 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | penetratin 12 | 1 |
Entities:
Entity 1, penetratin 12 12 residues - 1716 Da.
| 1 | ARG | GLN | ILE | LYS | ILE | TRP | PHE | ARG | LYS | TRP | ||||
| 2 | LYS | LYS |
Samples:
sample_1: 12 amino acid long derivative of the third helix of Antennapedia homeodomain 1.5 mM; trifluoroethanol 90%; water 10%
cond_set_1: pH: 3; temperature: 300 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H DQF-COSY | not available | not available | not available |
| 2D 1H-1H TOCSY | not available | not available | not available |
| 2D 1H-1H NOESY | not available | not available | not available |
Software:
FELIX v97.2 - peak assignment, peak picking, raw spectral data processing
NMR spectrometers:
- Bruker DRX 500 MHz