BMRB Entry 5486
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5486
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Title: Backbone and 1H assignments for Tachyplesin I, wild type
Deposition date: 2002-08-02 Original release date: 2002-11-04
Authors: Laederach, Alain; Andreotti, Amy; Fulton, Donald
Citation: Laederach, Alain; Andreotti, Amy; Fulton, Donald. "Solution and micelle-bound structures of tachyplesin I and its active aromatic linear derivatives" Biochemistry 41, 12359-12368 (2002).
Assembly members:
Tachyplesin I, polymer, 17 residues, Formula weight is not available
Natural source: Common Name: Horseshoe crab Taxonomy ID: 6853 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Tachypleus tridentatus
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
Tachyplesin I: KWCFRVCYRGICYRRCR
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 198 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Tachyplesin I, Wild type | 1 |
Entities:
Entity 1, Tachyplesin I, Wild type 17 residues - Formula weight is not available
| 1 | LYS | TRP | CYS | PHE | ARG | VAL | CYS | TYR | ARG | GLY | ||||
| 2 | ILE | CYS | TYR | ARG | ARG | CYS | ARG |
Samples:
water_sample: Tachyplesin I0.5 – 1.0 mM; TFA 0.15%
DPC_micelle_sample: Tachyplesin I 0.5 mM; TFA 0.15%; Dodecylphosphocholine, [U-98% D], 320 mM
condition_Water_4C: pH: 3.0; temperature: 277 K; ionic strength: 0.0015 %
condition_Water_25C: pH: 3.0; temperature: 298 K; ionic strength: 0.0015 %
condition_DPC_40C: pH: 3.0; temperature: 313 K; ionic strength: 0.0015 %
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | not available | not available | not available |
| 2D 1H-1H TOCSY | not available | not available | not available |
| 2D 1H-1H ROESY | not available | not available | not available |
Software:
No software information available
NMR spectrometers:
- Bruker DRX 500 MHz