BMRB Entry 5911
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5911
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Title: NMR Solution Structure of a Peptide from the mdm-2 Binding Domain of the p53 Protein that is Selectively Cytotoxic to Cancer Cells PubMed: 14967026
Deposition date: 2003-08-20 Original release date: 2004-03-07
Authors: Rosal, R.; Pincus, M.; Brandt-Rauf, P.; Fine, R.; Wang, H.
Citation: Rosal, R.; Pincus, M.; Brandt-Rauf, P.; Fine, R.; Michl, J.; Wang, H.. "NMR Solution Structure of a Peptide from the mdm-2 Binding Domain of the p53 Protein that is Selectively Cytotoxic to Cancer Cells" Biochemistry 43, 1854-1861 (2004).
Assembly members:
PNC27, polymer, 32 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
PNC27: PPLSQETFSDLWKLLKKWKM
RRNQFWVKVQRG
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 112 |
| 1H chemical shifts | 228 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | PNC27 | 1 |
Entities:
Entity 1, PNC27 32 residues - Formula weight is not available
| 1 | PRO | PRO | LEU | SER | GLN | GLU | THR | PHE | SER | ASP | ||||
| 2 | LEU | TRP | LYS | LEU | LEU | LYS | LYS | TRP | LYS | MET | ||||
| 3 | ARG | ARG | ASN | GLN | PHE | TRP | VAL | LYS | VAL | GLN | ||||
| 4 | ARG | GLY |
Samples:
sample_1: PNC27 4 mM; DMSO-d6 5%; sodium phosphate 10 mM; H2O 95%
sample_cond_1: ionic strength: 10 mM; pH: 5.7; pressure: 1 atm; temperature: 310 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | not available | not available |
| 2D TOCSY | not available | not available | not available |
| DQF-COSY | not available | not available | not available |
| 13C-HSQC | not available | not available | not available |
| 13C-HSQCTOCSY | not available | not available | not available |
Software:
NMRPipe v2001 - processing
NMRView v5.0.4 - data analysis
DYANA v1.5 - structure refinement, structure solution
NMR spectrometers:
- Varian INOVA 600 MHz
Related Database Links:
| PDB |