BMRB Entry 6085
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR6085
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Title: Solution Structure of hybrid white striped bass hepcidin PubMed: 15546886
Deposition date: 2004-01-28 Original release date: 2005-02-15
Authors: Babon, Jeff; Singh, Satenda; Westerman, Mark; Pennington, Mike; Norton, Raymond
Citation: Lauth, X.; Babon, Jeff; Stannard, J.; Singh, Satenda; Nizet, V.; Carlberg, J.; Ostland, V.; Pennington, M.; Norton, R.; Westerman, Mark. "Bass hepcidin: Synthesis, solution structure, antimicrobial activities and synergism, and in vivo hepatic response to bacterial infections" J. Biol. Chem. 280, 9272-9282 (2005).
Assembly members:
hepcidin, polymer, 21 residues, Formula weight is not available
Natural source: Common Name: hybrid white striped bass Taxonomy ID: 45352 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Morone chrysops x saxatilis
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
hepcidin: GCRFCCNCCPNMSGCGVCCR
F
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 59 |
| 15N chemical shifts | 9 |
| 1H chemical shifts | 113 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | hepcidin | 1 |
Entities:
Entity 1, hepcidin 21 residues - Formula weight is not available
| 1 | GLY | CYS | ARG | PHE | CYS | CYS | ASN | CYS | CYS | PRO | ||||
| 2 | ASN | MET | SER | GLY | CYS | GLY | VAL | CYS | CYS | ARG | ||||
| 3 | PHE |
Samples:
sample_1: hepcidin3 – 4 mM
condition_1: ionic strength: 0 mM; pH: 4.7; temperature: 298 K
condition_2: ionic strength: 0.01 mM; pH: 4.3; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H-1H TOCSY | not available | not available | not available |
| 1H-1H NOESY | not available | not available | not available |
| DQF-COSY | not available | not available | not available |
| E-COSY | not available | not available | not available |
| 15N-1H HSQC | not available | not available | not available |
| 13C-1H HSQC | not available | not available | not available |
Software:
xwinnmr -
xeasy -
nmrpipe -
x-plor-NIH -
NMR spectrometers:
- Bruker Avance 500 MHz
- Bruker DRX 600 MHz
Download simulated HSQC data in one of the following formats:
CSV: Backbone
or all simulated shifts
SPARKY: Backbone
or all simulated shifts