BMRB Entry 6155
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6155
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Title: 1H Assigned Chemical Shifts for FMBP-1 tandem repeat 4
Deposition date: 2004-03-22 Original release date: 2004-06-30
Authors: Kawaguchi, Kyosuke; Yamaki, Takeshi; Aizawa, Tomoyasu; Takiya, Shigeharu; Demura, Makoto; Nitta, Katsutoshi
Citation: Kawaguchi, Kyosuke; Yamaki, Takeshi; Aizawa, Tomoyasu; Takiya, Shigeharu; Demura, Makoto; Nitta, Katsutoshi. "1H Assigned Chemical Shifts for FMBP-1 tandem repeat 4" The BMRB entry is the only known published source for the data..
Assembly members:
fibroin-modulator-binding-protein-1, polymer, 23 residues, 2604 Da.
Natural source: Common Name: Silkworm Taxonomy ID: 7091 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Bombyx mori
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
fibroin-modulator-binding-protein-1: ETPAQRQARLLRMSAYAAKR
QAS
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 161 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | FMBP-1 | 1 |
Entities:
Entity 1, FMBP-1 23 residues - 2604 Da.
| 1 | GLU | THR | PRO | ALA | GLN | ARG | GLN | ALA | ARG | LEU | ||||
| 2 | LEU | ARG | MET | SER | ALA | TYR | ALA | ALA | LYS | ARG | ||||
| 3 | GLN | ALA | SER |
Samples:
sample_1: fibroin-modulator-binding-protein-1 1.5 mM
cond_1: pH: 4.0; temperature: 293 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| DQF-COSY | sample_1 | not available | cond_1 |
| TOCSY | sample_1 | not available | cond_1 |
| NOESY | sample_1 | not available | cond_1 |
Software:
NMRPipe - raw spectral data processing
XEASY - peak picking, assignments
NMR spectrometers:
- Bruker DRX 600 MHz
- Jeol ALPHA 600 MHz