BMRB Entry 6200
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6200
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Title: Assignment of the minicollagen 1 cysteine rich domain PubMed: 15225618
Deposition date: 2004-04-29 Original release date: 2004-09-07
Authors: Meier, Sebastian; Grzesiek, Stephan
Citation: Meier, Sebastian; Haussinger, Daniel; Pokidysheva, Elena; Bachinger, Hans; Grzesiek, Stephan. "Determination of a high-precision NMR structure of the minicollagen cysteine rich domain from Hydra and characterization of its disulfide bond formation" FEBS Lett. 569, 112-116 (2004).
Assembly members:
MCRD, polymer, 24 residues, Formula weight is not available
Natural source: Common Name: Hydra Taxonomy ID: 6083 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Hydra not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
MCRD: PCPPVCVAQCVPTCPQYCCP
AKRK
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 83 |
| 15N chemical shifts | 20 |
| 1H chemical shifts | 161 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | MCRD_1 | 1 |
Entities:
Entity 1, MCRD_1 24 residues - Formula weight is not available
| 1 | PRO | CYS | PRO | PRO | VAL | CYS | VAL | ALA | GLN | CYS | ||||
| 2 | VAL | PRO | THR | CYS | PRO | GLN | TYR | CYS | CYS | PRO | ||||
| 3 | ALA | LYS | ARG | LYS |
Samples:
sample_1: MCRD 5 mM
Ex-cond_1: pH: 6.5; pressure: 1 atm; temperature: 288 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| homonuclear NOESY | sample_1 | not available | Ex-cond_1 |
| TOCSY | sample_1 | not available | Ex-cond_1 |
| nat. abundance 13C-HMQC | sample_1 | not available | Ex-cond_1 |
| 13C-HMBC | sample_1 | not available | Ex-cond_1 |
| 15N-HSQC | sample_1 | not available | Ex-cond_1 |
Software:
nmrpipe - .
NMR spectrometers:
- Bruker DRX 600 MHz
- Bruker DRX 800 MHz
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