BMRB Entry 6245
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6245
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Title: Solution Structure of GIP(1-30)amide in TFE/Water PubMed: 15522230
Deposition date: 2004-06-23 Original release date: 2008-07-16
Authors: Alana, I.; Hewage, C.; Malthouse, J.; Parker, J.; Gault, V.; O'Harte, F.
Citation: Alana, I.; Hewage, C.; Malthouse, J.; Parker, J.; Gault, V.; O'Harte, F.. "NMR structure of the glucose-dependent insulinotropic polypeptide fragment, GIP(1-30)amide" Biochem. Biophys. Res. Commun. 325, 281-286 (2004).
Assembly members:
Gastric inhibitory polypeptide, polymer, 31 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
Gastric inhibitory polypeptide: YAEGTFISDYSIAMDKIHQQ
DFVNWLLAQKX
- assigned_chemical_shifts
- coupling_constants
| Data type | Count |
| 1H chemical shifts | 79 |
| coupling constants | 16 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Gastric inhibitory polypeptide | 1 |
Entities:
Entity 1, Gastric inhibitory polypeptide 31 residues - Formula weight is not available
| 1 | TYR | ALA | GLU | GLY | THR | PHE | ILE | SER | ASP | TYR | ||||
| 2 | SER | ILE | ALA | MET | ASP | LYS | ILE | HIS | GLN | GLN | ||||
| 3 | ASP | PHE | VAL | ASN | TRP | LEU | LEU | ALA | GLN | LYS | ||||
| 4 | NH2 |
Samples:
sample_1: Gastric inhibitory polypeptide 2 mM; H2O 50%; d3-TFE 50%
sample_cond_1: pH: 3.0; temperature: 298 K; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| DQF-COSY | sample_1 | not available | sample_cond_1 |
| 2D TOCSY | sample_1 | not available | sample_cond_1 |
| 2D NOESY | sample_1 | not available | sample_cond_1 |
| 1D variable temperature | sample_1 | not available | sample_cond_1 |
| 1D D2O exchange | sample_1 | not available | sample_cond_1 |
Software:
XWINNMR v3.5 - collection, processing
SYBYL v6.81 - data analysis, refinement
CYANA v1.0.6 - structure solution
NMR spectrometers:
- Bruker DRX 900 MHz
Related Database Links:
| BMRB | 17330 17331 6681 |
| PDB | |
| GB | AAA53192 AAA88043 AAH69100 AAH69663 AAH69686 |
| REF | NP_004114 XP_001091383 XP_001172671 XP_002806900 XP_003278797 |
| SP | P09681 |