BMRB Entry 5346
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5346
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Title: Solution Structure of a Novel Disintegrin, Salmosin from Agkistrondon halys Venom PubMed: 14661951
Deposition date: 2002-04-19 Original release date: 2004-02-12
Authors: Shin, Joon; Hong, Sung-Yu; Chung, Kwanghoe; Kang, Incheol; Jang, Yangsoo; Kim, Doo-sik; Lee, Weontae
Citation: Shin, Joon; Hong, Sung-Yu; Chung, Kwanghoe; Kang, Incheol; Jang, Yangsoo; Kim, Doo-sik; Lee, Weontae. "Solution Structure of a Novel Disintegrin, Salmosin from Agkistrondon halys Venom" Biochemistry 42, 14408-14415 (2003).
Assembly members:
salmosin, polymer, 73 residues, Formula weight is not available
Natural source: Common Name: Korean snake Taxonomy ID: 8714 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Agkistrondon halys
Experimental source: Production method: purified from the natural source
Entity Sequences (FASTA):
salmosin: EAGEECDCGSPGNPCCDAAT
CKLRQGAQCAEGLCCDQCRF
MKEGTICRRARGDDLDDYCN
GISAGCPRNPFHA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 391 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | platelet aggregation inhibitor disintegrin | 1 |
Entities:
Entity 1, platelet aggregation inhibitor disintegrin 73 residues - Formula weight is not available
| 1 | GLU | ALA | GLY | GLU | GLU | CYS | ASP | CYS | GLY | SER | ||||
| 2 | PRO | GLY | ASN | PRO | CYS | CYS | ASP | ALA | ALA | THR | ||||
| 3 | CYS | LYS | LEU | ARG | GLN | GLY | ALA | GLN | CYS | ALA | ||||
| 4 | GLU | GLY | LEU | CYS | CYS | ASP | GLN | CYS | ARG | PHE | ||||
| 5 | MET | LYS | GLU | GLY | THR | ILE | CYS | ARG | ARG | ALA | ||||
| 6 | ARG | GLY | ASP | ASP | LEU | ASP | ASP | TYR | CYS | ASN | ||||
| 7 | GLY | ILE | SER | ALA | GLY | CYS | PRO | ARG | ASN | PRO | ||||
| 8 | PHE | HIS | ALA |
Samples:
sample_1: salmosin 1.0 mM; H2O 90%; D2O 10%
experimental_conditions: ionic strength: 50 mM; pH: 7; pressure: 1 atm; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | not available | not available |
| DQF-COSY | not available | not available | not available |
| 2D TOCSY | not available | not available | not available |
Software:
XWINNMR v2.6 - collection, processing
CNS v1.0 - refinement
Sparky v3.1 - data analysis
NMR spectrometers:
- Bruker DRX 600 MHz
- Bruker DRX 500 MHz