BMRB Entry 5454
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5454
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Title: NMR solution structure and dynamics of motilin in isotropic phospholipid bicellar solution
Deposition date: 2002-07-03 Original release date: 2002-11-06
Authors: Andersson, August; Maler, Lena
Citation: Andersson, August; Maler, Lena. "NMR solution structure and dynamics of motilin in isotropic phospholipid bicellar solution" J. Biomol. NMR 24, 103-112 (2002).
Assembly members:
motilin, polymer, 22 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
motilin: FVPIFTYGELQRMQEKERNK
GQ
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 141 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | motilin subunit 1 | 1 |
Entities:
Entity 1, motilin subunit 1 22 residues - Formula weight is not available
| 1 | PHE | VAL | PRO | ILE | PHE | THR | TYR | GLY | GLU | LEU | ||||
| 2 | GLN | ARG | MET | GLN | GLU | LYS | GLU | ARG | ASN | LYS | ||||
| 3 | GLY | GLN |
Samples:
sample_1: motilin 3 mM; DMPG 24 mM; DMPC 74 mM; DHPC 192 mM
cond_1: pH: 5.5; temperature: 310 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H-1H NOESY | not available | not available | not available |
| 1H-1H TOCSY | not available | not available | not available |
Software:
Felix v97.0 - assignments
NMR spectrometers:
- Varian INOVA 600 MHz
- Varian INOVA 800 MHz
Related Database Links:
| BMRB | 754 |
| PDB | |
| EMBL | CAA33448 CAA68690 |
| GB | AAA59860 AAH69675 AAI12315 AAI43982 AAY53628 |
| REF | NP_001035198 NP_001171627 NP_002409 XP_002816813 XP_002816814 |
| SP | P01307 P12872 |